Sonoma State University
Chemistry 335A
Spring 2004
Instructor: Dale Trowbridge
LABORATORY SCHEDULE
TEXT: The Organic Chemistry Lavoratory Survival
Manual, 5th ed., by James W. Zubrick
OTHER REQUIRED MATERIALS: Safety glasses
| Wednesday Lab | Thursday Lab | Experiment | Reading Assignment |
| Jan. 28 | Jan. 29 | Check in, Safety Lecture, Library Exercise: 10 pts; Hydrolysis of MethylBenzoate 10 pts | Chapter 1, 2, 3, 22 |
| Feb. 4 | Feb. 5 | Recrystallization and Melting Point of Benzoic Acid from Lab 1: 10 pts | Chapter 13 |
| Feb. 11 | Feb. 12 | Extraction and Chromatography of Organic Mixtures: 10 pts | Handout; Chapters 26, 27, 28, 30 |
| Feb. 18 | Feb. 19 | Simple and Fractional Distillation and Gas Liquid Chromatography of an Ethyl Acetate/Butyl Acetate Mixture: 15 pts | Handout; Chapters 20, 35, 31 |
| Feb. 24 | Feb. 25 | Steam Distillation and Extraction of a Natural Product; GLPC Analysis of Product; Refractive Index | Handout; Chapters 15, 31, 29 |
| March 3 | March 4 | Infrared Spectrum and Nuclear Magnetic Resonance Spectrum and Mass Spectrum of natural Oil (total of 30 pts) | Handout; Chapter 34 |
| March 10, 17, 24 | Mar. 11, 18, 25 | Active Extraction Identification of Organic Unknowns: 40 pts |
Chapter 15 |
| April 14 | April 15 | Kinetics I: Solvolysis of an Alkyl Halide: 15 pts | |
| Apr. 21, 28 | Apr. 22, 29 | Oxidation of a Secondary Alcohol: 20 pts Functional Group Interconversions (FGI) |
Handout |
| May 5 | May 6 | Kinetics II: Nucleophilic Substituiton of a PRimary Alkyl Halide: 15 pts | |
| May 12 | May 13 | Final, Check out |
Grading: laboratory Reports and Products
- 175 points
Laboratory Examination - 75 points
TOTAL POINTS = 250 points